2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide

Base Information

• Chemical Name: 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide
• CAS No.: 117897-72-0
• Molecular Formula: C₁₉H₈F₂₀N₂O
• Molecular Weight: 660.253

Synonyms:2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide

Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide

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Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide

There total 2 articles about 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

11-hydroperfluoroundecanoic acid (1765-48-6) → 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide (117897-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl acetate / 15 h / 85 °C

2: 5.1 g / ethyl acetate / 24 h / Ambient temperature

In ethyl acetate;

DOI:10.1021/jm00083a021

Reference yield:

p-aminophenylacetonitrile (3544-25-0) + 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-Icosafluoro-undecanoic acid 1-ethoxy-vinyl ester → 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide (117897-72-0)

Guidance literature:

In ethyl acetate; for 24h; Ambient temperature;

DOI:10.1021/jm00083a021

Reference yield: 51.0%

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(cyanomethyl)phenyl>undecanamide (117897-72-0) → 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(1H-tetrazol-5-ylmethyl)phenyl>undecanamide (117293-65-9)

Guidance literature:

With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 135 ℃; for 18h;

DOI:10.1021/jm00083a021

upstream raw materials:

p-aminophenylacetonitrile

11-hydroperfluoroundecanoic acid

Downstream raw materials:

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11-eicosafluoro-N-<4-(1H-tetrazol-5-ylmethyl)phenyl>undecanamide

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