3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

Base Information

Chemical Name:3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on
CAS No.:121868-77-7
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

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Chemical Property of 3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

Chemical Property:

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Technology Process of 3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

There total 5 articles about 3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 121868-70-0
3-<<<2,5-Bis(benzyloxy)-4-methylphenyl>methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

: 121868-77-7
3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 760 Torr; Ambient temperature;

Reference yield:

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

: 121868-77-7
3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / ethanol / 1 h / Heating

2: 93 percent / LiAlH₄ / diethyl ether / 48 h / Ambient temperature

3: 89 percent / p-toluenesulfonic acid / toluene / Heating

4: 68 percent / H₂ / 10percent Pd-C / tetrahydrofuran / 760 Torr / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; toluene;

Reference yield:

: 126-81-8
dimedone

: 121868-77-7
3-<<(2,5-Dihydroxy-4-methylphenyl)methyl>methylamino>-5,5-dimethyl-2-cyclohexen-1-on

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / p-toluenesulfonic acid / toluene / Heating

2: 68 percent / H₂ / 10percent Pd-C / tetrahydrofuran / 760 Torr / Ambient temperature

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; toluene;