3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

Base Information

Chemical Name:3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole
CAS No.:339064-34-5
Molecular Formula:C₄₈H₇₁N₇
Molecular Weight:746.139
Hs Code.:

Synonyms:3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

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Chemical Property of 3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

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Technology Process of 3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

There total 8 articles about 3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 339064-30-1
4-amino-3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

: 339064-34-5
3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

Guidance literature:: With hydrogenchloride; sodium nitrite; In ethanol; at -10 - 20 ℃; for 5h;
DOI:10.1021/jo0056794

Reference yield:

: 79073-01-1
4,5-dibutyl-1H-imidazole

: 339064-34-5
3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / KOH / acetonitrile; dioxane / 17 h / Heating

2: 96 percent / SOCl₂ / CH₂Cl₂ / 5 h / 20 °C

3: 88 percent / dimethylformamide / 24 h / 80 °C

4: 73 percent / hydrazine hydrate / 18 h / 100 - 170 °C

5: 89 percent / aq. HCl; NaNO₂ / ethanol / 5 h / -10 - 20 °C

With hydrogenchloride; potassium hydroxide; thionyl chloride; hydrazine hydrate; sodium nitrite; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo0056794

Reference yield:

: 22157-91-1
1,3-bis(hydroxymethyl)-5-tert-butylbenzene

: 339064-34-5
3,5-bis[[[3-tert-butyl-5-(4,5-dibutylimidazolyl)methyl]phenyl]methyl]-1,2,4-triazole

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / HBr conc. / 5 h / 20 °C

2: 84 percent / KOH / acetonitrile; dioxane / 17 h / Heating

3: 96 percent / SOCl₂ / CH₂Cl₂ / 5 h / 20 °C

4: 88 percent / dimethylformamide / 24 h / 80 °C

5: 73 percent / hydrazine hydrate / 18 h / 100 - 170 °C

6: 89 percent / aq. HCl; NaNO₂ / ethanol / 5 h / -10 - 20 °C

With hydrogenchloride; potassium hydroxide; thionyl chloride; hydrogen bromide; hydrazine hydrate; sodium nitrite; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo0056794