tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

Base Information

Chemical Name:tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate
CAS No.:1252933-98-4
Molecular Formula:C₂₅H₃₈N₆O₅
Molecular Weight:502.614
Hs Code.:

Synonyms:tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

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Chemical Property of tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

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Technology Process of tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

There total 1 articles about tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 584-13-4
4-amino-1,2,4-triazole

: 210355-26-3
3,5-Bis-(3-tert-butoxycarbonylamino-propyl)-benzoic acid

: 1252933-98-4
tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

Guidance literature:: With diphenyl (2,3-dihydro-2-thioxo-3-benzoxazolyl)phosphonate; triethylamine; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1002/ejic.201000067

Reference yield: 94.0%

: iron (II) p-toluenesulphonate hexahydrate

: 1252933-98-4
tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

: [Fe(tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate)][tosylate]2

Guidance literature:: With ascorbic acid; In methanol; soln. of Fe compd. (0.13 mmol) and ascorbic acid in MeOH added droppwiseto MeOH soln. of ligand (0.4 mmol) at 60°C with stirring, stirre d for 1 h; cooled to room temp., evapd., washed (MeOH, THF), dried (vac.), elem. anal.;
DOI:10.1002/ejic.201000067

Reference yield: 93.0%

: iron(II) trifluoromethanesulfonate hexahydrate

: 1252933-98-4
tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate

: [Fe(tert-butyl-[3-[3-(3-tert-butoxycarbonylaminopropyl)-5-([1,2,4]triazol-4-ylcarbamoyl)phenyl]propyl]carbamate)][triflate]2

Guidance literature:: With ascorbic acid; In methanol; soln. of Fe compd. (0.13 mmol) and ascorbic acid in MeOH added droppwiseto MeOH soln. of ligand (0.4 mmol) at 60°C with stirring, stirre d for 1 h; cooled to room temp., evapd., washed (MeOH, THF), dried (vac.), elem. anal.;
DOI:10.1002/ejic.201000067