Technology Process of C25H30N2O
There total 5 articles about C25H30N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(acetylacetonate)nickel(II); o-phenylenebis(diphenylphosphine); caesium carbonate; cesium iodide;
In
toluene;
at 150 ℃;
for 24h;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/ja413131m
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 17 h / 0 - 20 °C
2: triethylamine / dichloromethane / 20 °C
3: bis(acetylacetonate)nickel(II); o-phenylenebis(diphenylphosphine); caesium carbonate; cesium iodide / toluene / 24 h / 150 °C / Schlenk technique; Inert atmosphere
With
bis(acetylacetonate)nickel(II); oxalyl dichloride; o-phenylenebis(diphenylphosphine); caesium carbonate; triethylamine; cesium iodide;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja413131m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 20 °C
2: bis(acetylacetonate)nickel(II); o-phenylenebis(diphenylphosphine); caesium carbonate; cesium iodide / toluene / 24 h / 150 °C / Schlenk technique; Inert atmosphere
With
bis(acetylacetonate)nickel(II); o-phenylenebis(diphenylphosphine); caesium carbonate; triethylamine; cesium iodide;
In
dichloromethane; toluene;
DOI:10.1021/ja413131m
