1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride

Base Information

Chemical Name:1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride
CAS No.:96441-91-7
Molecular Formula:C₉H₁₀ClN₃*ClH
Molecular Weight:232.112
Hs Code.:2933990090
European Community (EC) Number:970-405-3
DSSTox Substance ID:DTXSID20532479
Mol file:96441-91-7.mol

Synonyms:1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride;96441-91-7;4-chloro-5,6,7-trimethylpyrrolo[3,4-d]pyridazine;hydrochloride;DTXSID20532479;AKOS026726335;CS-0243611;EN300-26626;G24148;3-(AMINOCARBONYL)-1,4-DIMETHYLPYRIDINIUMCHLORIDE;Z235344811;1-Chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine--hydrogen chloride (1/1)

Suppliers and Price of 1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-CHLORO-5,6,7-TRIMETHYL-6H-PYRROLO[3,4-D]PYRIDAZINE HYDROCHLORIDE 95.00%
2.5G
$ 1147.43

American Custom Chemicals Corporation
1-CHLORO-5,6,7-TRIMETHYL-6H-PYRROLO[3,4-D]PYRIDAZINE HYDROCHLORIDE 95.00%
1G
$ 402.15

Total 5 raw suppliers

Chemical Property of 1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride

Chemical Property:

PSA：30.71000
LogP:3.04050
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:231.0330028
Heavy Atom Count:14
Complexity:199

Purity/Quality:

97% ^*data from raw suppliers

1-CHLORO-5,6,7-TRIMETHYL-6H-PYRROLO[3,4-D]PYRIDAZINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C=NN=C(C2=C(N1C)C)Cl.Cl

Technology Process of 1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride

There total 3 articles about 1-chloro-5,6,7-trimethyl-6H-pyrrolo[3,4-d]pyridazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 90817-87-1
1,2-dihydro-5,6,7-trimethyl-6H-pyrrolo<3,4-d>pyridazine-1-one

: 96441-91-7
1-chloro-5,6,7-trimethyl-6H-pyrrolo<3,4-d>pyridazinium chloride

Guidance literature:: With trichlorophosphate; at 85 ℃; for 4h;
DOI:10.1016/0040-4020(84)85076-0

Reference yield:

: 776-24-9
ethyl 4-formyl-2, 5-dimethyl-1H-pyrrole-3-carboxylate

: 96441-91-7
1-chloro-5,6,7-trimethyl-6H-pyrrolo<3,4-d>pyridazinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH, tetrabutylammonium bromide / CH₂Cl₂ / 3 h / 0 °C

2: 83 percent / hydrazine hydrate / ethanol / Heating

3: 71 percent / POCl₃ / 4 h / 85 °C

With sodium hydroxide; tetrabutylammomium bromide; hydrazine hydrate; trichlorophosphate; In ethanol; dichloromethane;
DOI:10.1016/0040-4020(84)85076-0

Reference yield:

: 63050-13-5
ethyl 4-formyl-1,2,5-trimethyl-1H-pyrrole-3-carboxylate

: 96441-91-7
1-chloro-5,6,7-trimethyl-6H-pyrrolo<3,4-d>pyridazinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / hydrazine hydrate / ethanol / Heating

2: 71 percent / POCl₃ / 4 h / 85 °C

With hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1016/0040-4020(84)85076-0