ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate

Base Information

• Chemical Name: ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate
• CAS No.: 149727-89-9
• Molecular Formula: C₂₂H₂₁F₅N₄O₄
• Molecular Weight: 500.425

Synonyms:ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate

Chemical Property of ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate

There total 2 articles about ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[[4-(aminoiminomethyl)phenyl]amino]-4-oxobutanoic acid, monohydrochloride → ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate (149727-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide / 0.08 h / 25 °C

2: DMAP, diisopropylethylamine / dimethylformamide / 1 h

With 4-methyl-morpholine; dmap; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/jm00013a014

Reference yield:

ethyl 3-amino-3-(pentafluorophenyl)propanoate + C16H21N3O5 (1027293-42-0) → ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate (149727-89-9)

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h;

DOI:10.1021/jm00013a014

Reference yield:

ethyl β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoate (149727-89-9) → β-<<4-<<4-(aminoiminomethyl)phenyl>amino>-1,4-dioxobutyl>amino>-3-(pentafluorophenyl)propanoic acid

Guidance literature:

With lithium hydroxide; In acetonitrile; at 25 ℃; for 0.5h;

DOI:10.1021/jm00013a014

upstream raw materials:

C₁₆H₂₁N₃O₅

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