(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

Base Information

Chemical Name:(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester
CAS No.:1003309-24-7
Molecular Formula:C₂₇H₂₃NO₅
Molecular Weight:441.483
Hs Code.:

Synonyms:(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

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Chemical Property of (E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

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Technology Process of (E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

There total 3 articles about (E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1003309-23-6
(E)-3-phenylacrylic acid 4-[(E)-(3-phenylacryloyl)amino]phenyl ester

: 96-32-2
bromoacetic acid methyl ester

: 1003309-24-7
(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 72h;

Reference yield:

: 123-30-8
4-amino-phenol

: 1003309-24-7
(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 2.5 h / 20 °C

2: sodium hydride / tetrahydrofuran / 72 h / 20 °C

With pyridine; dmap; sodium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 1003309-24-7
(E)-3-phenylacrylic acid 4-{methoxycarbonylmethyl-[(E)-3-phenylacryloyl]-amino}phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 2.5 h / 20 °C

2: sodium hydride / tetrahydrofuran / 72 h / 20 °C

With pyridine; dmap; sodium hydride; In tetrahydrofuran; dichloromethane;