4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one

Base Information

• Chemical Name: 4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one
• CAS No.: 35847-75-7
• Molecular Formula: C₂₄H₂₂N₆O₇
• Molecular Weight: 506.475

Synonyms:4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one

Chemical Property of 4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one

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Technology Process of 4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one

There total 2 articles about 4-amino-1-(4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetylamino-1-(O6-acetyl-4-azido-O2,O3-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one (35847-73-5) → 4-amino-1-(4-azido-O2,O3-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one (35847-75-7)

Guidance literature:

With triethylamine; In methanol; at 20 ℃; for 48h;

DOI:10.1021/ol0507322

Reference yield:

→ 4-amino-1-(4-azido-O2,O3-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one (35847-75-7)

Guidance literature:

Verb. (10), Et3N;

DOI:10.1016/S0008-6215(00)81740-1

Reference yield:

4-amino-1-(4-azido-O2,O3-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one (35847-75-7) → (2S,3S,4S,5R,6R)-6-(4-Amino-2-oxo-2H-pyrimidin-1-yl)-3-azido-4,5-bis-benzoyloxy-tetrahydro-pyran-2-carboxylic acid (575457-74-8)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; water; In acetonitrile; at 20 ℃; for 4h;

DOI:10.1021/ol0507322

upstream raw materials:

4-acetylamino-1-(O⁶-acetyl-4-azido-O²,O³-dibenzoyl-β-D-4-deoxy-glucopyranosyl)-1H-pyrimidin-2-one

Downstream raw materials:

(2S,3S,4S,5R,6R)-6-(4-Amino-2-oxo-2H-pyrimidin-1-yl)-3-azido-4,5-bis-benzoyloxy-tetrahydro-pyran-2-carboxylic acid

(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-[2-oxo-4-(2-trimethylsilanyl-ethoxycarbonylamino)-2H-pyrimidin-1-yl]-tetrahydro-pyran-2-carboxylic acid

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