4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

Base Information

Chemical Name:4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside
CAS No.:108512-29-4
Molecular Formula:C₂₇H₂₉NO₁₀
Molecular Weight:527.528
Hs Code.:

Synonyms:4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

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Chemical Property of 4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

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Technology Process of 4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

There total 1 articles about 4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5307-05-1
1-hydroxy-4-methoxy-2-methylbenzene

: 108512-26-1
acetyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-glucopyranoside

: 108512-30-7
4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-β-D-glucopyranoside

: 108512-29-4
4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 23 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00392a013

Reference yield: 100.0%

: 108512-29-4
4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

: 108512-31-8
4-methoxy-2-methylphenyl 3-deoxy-2-methoxy-3-phthalimido-α-D-glucopyranoside

Guidance literature:: With potassium carbonate; In methanol; at 23 ℃; for 2h;
DOI:10.1021/jo00392a013

Reference yield:

: 108512-29-4
4-methoxy-2-methylphenyl 4,6-di-O-acetyl-3-deoxy-2-methoxy-3-phthalimido-α-D-dlucopyranoside

: 108512-32-9
4-methoxy-2-methylphenyl 3-deoxy-6-<(methylsulfonyl)oxy>-2-methoxy-3-phthalimido-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / K₂CO₃ / methanol / 2 h / 23 °C

2: 98 percent / pyridine / 48 h / 0 °C

With pyridine; potassium carbonate; In methanol;
DOI:10.1021/jo00392a013