Technology Process of Benzoyl chloride, 4,5-dimethoxy-2-methyl- (9CI)
There total 5 articles about Benzoyl chloride, 4,5-dimethoxy-2-methyl- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; oxalyl dichloride;
In
dichloromethane;
for 2h;
DOI:10.1021/jo00245a052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 91 percent / silver oxide, aq. sodium hydroxide / ethanol / 50 - 60 °C
2: pyridine, oxalyl chloride / CH2Cl2 / 2 h
With
pyridine; sodium hydroxide; oxalyl dichloride; silver(l) oxide;
In
ethanol; dichloromethane;
DOI:10.1021/jo00245a052
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) n-butyllithium / 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 1 h
2: 91 percent / 10percent HCl / tetrahydrofuran / Ambient temperature
3: 91 percent / silver oxide, aq. sodium hydroxide / ethanol / 50 - 60 °C
4: pyridine, oxalyl chloride / CH2Cl2 / 2 h
With
pyridine; hydrogenchloride; sodium hydroxide; n-butyllithium; oxalyl dichloride; silver(l) oxide;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00245a052
