3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

Base Information

Chemical Name:3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester
CAS No.:350817-32-2
Molecular Formula:C₃₈H₆₉NO₆Si
Molecular Weight:664.054
Hs Code.:

3-benzyloxy-2-<i>tert</i>-butoxycarbonylamino-propionic acid 1-[2-(<i>tert</i>-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

Synonyms:3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

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Chemical Property of 3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

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Technology Process of 3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

There total 6 articles about 3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 23680-31-1
BOC-O-benzyl-L-serine

: 350817-18-4
(2R,3R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-methyl-hexadecan-3-ol

: 350817-32-2
3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide;
DOI:10.1055/s-2001-13382

Reference yield:

: 124-25-4,511542-15-7
myristylaldehyde

: 350817-32-2
3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: n-Bu₂BOTf; Et₃N

2: LiOH; H₂O₂

3: 99 percent / LiBH₄ / methanol

4: 86 percent / Et₃N; DMAP

5: 100 percent / DCC; HOBt

With dmap; lithium hydroxide; lithium borohydride; di-n-butylboryl trifluoromethanesulfonate; dihydrogen peroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1055/s-2001-13382

Reference yield:

: 350817-17-3
(2S,3R)-3-Hydroxy-2-methyl-hexadecanoic acid methyl ester

: 350817-32-2
3-benzyloxy-2-tert-butoxycarbonylamino-propionic acid 1-[2-(tert-butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-tetradecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / LiBH₄ / methanol

2: 86 percent / Et₃N; DMAP

3: 100 percent / DCC; HOBt

With dmap; lithium borohydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1055/s-2001-13382