9--6-(4-chlorophenylsulfanyl)-9H-purine

Base Information

Chemical Name:9--6-(4-chlorophenylsulfanyl)-9H-purine
CAS No.:172324-63-9
Molecular Formula:C₂₃H₂₁ClN₄OS
Molecular Weight:436.965
Hs Code.:

9-<cis-3-(benzyloxymethyl)cyclobutyl>-6-(4-chlorophenylsulfanyl)-9H-purine

Synonyms:9--6-(4-chlorophenylsulfanyl)-9H-purine

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Chemical Property of 9--6-(4-chlorophenylsulfanyl)-9H-purine

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Technology Process of 9--6-(4-chlorophenylsulfanyl)-9H-purine

There total 8 articles about 9--6-(4-chlorophenylsulfanyl)-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5457-98-7
6-(4-chlorophenylsulfanyl)-9H-purine

: 172324-65-1
(1r,3r)-3-((benzyloxy)methyl)cyclobutanol

: 172324-63-9
9--6-(4-chlorophenylsulfanyl)-9H-purine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1039/P19950002281

Reference yield:

: 14593-43-2
benzyl allyl ether

: 172324-63-9
9--6-(4-chlorophenylsulfanyl)-9H-purine

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / POCl₃, Zn-Cu couple / diethyl ether / 18 h / Heating

2: 68 percent / Zn, CH₃COOH / 4 h / Heating

3: L-Selectride / tetrahydrofuran / -78 °C

4: 88 percent / PPh₃, diethyl azodicarboxylate / tetrahydrofuran / 12 h / Ambient temperature

With L-Selectride; copper; acetic acid; triphenylphosphine; zinc; diethylazodicarboxylate; trichlorophosphate; In tetrahydrofuran; diethyl ether;
DOI:10.1039/P19950002281

Reference yield:

: 172324-66-2
3-(benzyloxymethyl)-2,2-dichlorocyclobutanone

: 172324-63-9
9--6-(4-chlorophenylsulfanyl)-9H-purine

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Zn, CH₃COOH / 4 h / Heating

2: L-Selectride / tetrahydrofuran / -78 °C

3: 88 percent / PPh₃, diethyl azodicarboxylate / tetrahydrofuran / 12 h / Ambient temperature

With L-Selectride; acetic acid; triphenylphosphine; zinc; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1039/P19950002281