1,4-ditritylbenzene

Base Information

Chemical Name:1,4-ditritylbenzene
CAS No.:103567-76-6
Molecular Formula:C₄₄H₃₄
Molecular Weight:562.754
Hs Code.:

Synonyms:1,4-ditritylbenzene

Suppliers and Price of 1,4-ditritylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-ditritylbenzene

Chemical Property:

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Technology Process of 1,4-ditritylbenzene

There total 4 articles about 1,4-ditritylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 103567-80-2
1,4-bis-(4-amino-trityl)-benzene

: 103567-76-6
1,4-ditritylbenzene

Guidance literature:: With hypophosphorous acid; acetic acid; sodium nitrite; In water; at 10 - 20 ℃; for 16h;
DOI:10.1002/ejoc.201201162

Reference yield:

: 57155-57-4
1,4-bis(diphenylhydroxymethyl)benzene

: 103567-76-6
1,4-ditritylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; acetic acid / 8 h / 140 °C

2: acetic acid; hypophosphorous acid; sodium nitrite / water / 16 h / 10 - 20 °C

With hydrogenchloride; hypophosphorous acid; acetic acid; sodium nitrite; In water;
DOI:10.1002/ejoc.201201162

Reference yield:

: 591-51-5
phenyllithium

: 103567-76-6
1,4-ditritylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: dibutyl ether; tetrahydrofuran / 17 h / -78 - 20 °C / Inert atmosphere

2: hydrogenchloride; acetic acid / 8 h / 140 °C

3: acetic acid; hypophosphorous acid; sodium nitrite / water / 16 h / 10 - 20 °C

With hydrogenchloride; hypophosphorous acid; acetic acid; sodium nitrite; In tetrahydrofuran; dibutyl ether; water;
DOI:10.1002/ejoc.201201162