Technology Process of C23H24(2)H2O9
There total 14 articles about C23H24(2)H2O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
W-2 Raney Ni;
In
ethanol;
at 25 ℃;
for 4h;
DOI:10.1021/jo00279a011
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) Br2, 2.) Dowex / 1.) HOAc, 2.) MeOH
2: 1.) n-BuLi / 1.) -78 deg C
3: DMAD / acetic acid
4: 100 percent / H2, K2CO3 / 10percent Pd/C / ethyl acetate / 6 h / 2585.7 Torr
5: 73 percent / H2 / W-2 Raney Ni / ethanol / 3 h / Heating
6: 1.) LiBEt3D, 2.) NaOMe / 1.) THF, 0 deg C, 1 h, 2.) CH3OH, 25 deg C, 1 h
With
lithium triethyl borodeuteride; n-butyllithium; dowex; hydrogen; bromine; sodium methylate; potassium carbonate;
palladium on activated charcoal; W-2 Raney Ni;
In
ethanol; acetic acid; ethyl acetate;
DOI:10.1021/jo00279a011
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) Br2, 2.) Dowex / 1.) HOAc, 2.) MeOH
2: 1.) n-BuLi / 1.) -78 deg C
3: DMAD / acetic acid
4: 100 percent / H2, K2CO3 / 10percent Pd/C / ethyl acetate / 6 h / 2585.7 Torr
5: 90 percent / NaOMe / methanol / 2 h / 25 °C
6: 1 M lithium triethylborodeuteride / tetrahydrofuran / 1 h / 0 °C
7: H2 / W-2 Raney Ni / ethanol / 4 h / 25 °C
With
lithium triethyl borodeuteride; n-butyllithium; dowex; hydrogen; bromine; sodium methylate; potassium carbonate;
palladium on activated charcoal; W-2 Raney Ni;
In
tetrahydrofuran; methanol; ethanol; acetic acid; ethyl acetate;
DOI:10.1021/jo00279a011
