Technology Process of C28H26O5S2
There total 5 articles about C28H26O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 ℃;
DOI:10.1021/ja00103a004
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) n-BuLi / 1.) THF, overnight, 2.) THF, a) RT, 2 h, b) 45 deg C, 3 d
2: 1.) KH / 1.) DMF, THF, -45 deg C, 30 min, 2.) DMF, THF, RT, overnight
3: 100 percent / tetrahydrofuran / 120 h / 8274370 Torr
4: 69 percent / MCPBA / CH2Cl2 / 0 °C
With
n-butyllithium; potassium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00103a004
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) KH / 1.) DMF, THF, -45 deg C, 30 min, 2.) DMF, THF, RT, overnight
2: 100 percent / tetrahydrofuran / 120 h / 8274370 Torr
3: 69 percent / MCPBA / CH2Cl2 / 0 °C
With
potassium hydride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00103a004