3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

Base Information

Chemical Name:3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile
CAS No.:29217-54-7
Molecular Formula:C₂₃H₁₇N₃O₃
Molecular Weight:383.406
Hs Code.:

3<i>t</i>-((9a<i>S</i>)-3-methyl-6,10-dioxo-1ξ-phenyl-(9a<i>r</i>)-9a,10-dihydro-6<i>H</i>,9<i>H</i>-2-oxa-6a,10a-diaza-benzo[<i>cd</i>]cyclopenta[<i>g</i>]azulen-8-yl)-acrylonitrile

Synonyms:3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

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Technology Process of 3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

There total 1 articles about 3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20998-79-2
3-(9-hydroxy-8-methyl-5,11-dioxo-5,10,11,11a-tetrahydro-1H-benzo[e]pyrrolo[1,2-a][1,4]diazepin-2-yl)-acrylonitrile

: 1125-88-8
benzaldehyde dimethyl acetal

: 29217-54-7
3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

Guidance literature:: at 200 ℃;
DOI:10.1021/ja01022a078

Reference yield:

: 29217-54-7
3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

: 29217-55-8
3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylamide

Guidance literature:: With PPA; water; at 95 ℃;
DOI:10.1021/ja01022a078

Reference yield:

: 29217-54-7
3t-((9aS)-3-methyl-6,10-dioxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylonitrile

: 20998-80-5
3t-((9aS)-10t-hydroxy-3-methyl-6-oxo-1ξ-phenyl-(9ar)-9a,10-dihydro-6H,9H-2-oxa-6a,10a-diaza-benzo[cd]cyclopenta[g]azulen-8-yl)-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: polyphosphoric acid, H₂O / 95 °C

2: NaBH₄ / methanol / 5 °C

With sodium tetrahydroborate; PPA; water; In methanol;
DOI:10.1021/ja01022a078