C₄₁H₅₆O₁₀

Base Information Edit

Chemical Name:C₄₁H₅₆O₁₀
CAS No.:474125-39-8
Molecular Formula:C₄₁H₅₆O₁₀
Molecular Weight:708.89
Hs Code.:
Mol file:474125-39-8.mol

C<sub>41</sub>H<sub>56</sub>O<sub>10</sub>

Synonyms:C₄₁H₅₆O₁₀

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Chemical Property of C₄₁H₅₆O₁₀ Edit

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Technology Process of C₄₁H₅₆O₁₀

There total 24 articles about C₄₁H₅₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3587-60-8
Benzyloxymethyl chloride

: 474125-38-7
C₃₃H₄₈O₉

: 474125-39-8
C₄₁H₅₆O₁₀

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 40 ℃; for 14h;
DOI:10.1016/S0040-4020(02)00660-9

Reference yield:

: 196393-04-1
(3S,4S,5R,6S)-6-Benzyloxymethyl-5-hydroxy-3,4-dimethyl-tetrahydro-pyran-2-one

: 474125-39-8
C₄₁H₅₆O₁₀

Guidance literature:: Multi-step reaction with 21 steps

1.1: 95 percent / N,N-diisopropylethylamine / 1,2-dichloro-ethane / 24 h / 50 °C

2.1: tetrahydrofuran / 1.17 h / -70 °C

3.1: disiamylborane / tetrahydrofuran / 1.17 h / 0 °C

3.2: H₂O₂; NaHCO₃ / tetrahydrofuran; methanol; H₂O / 20 °C

4.1: 37.5 g / 10-camphorsulfonic acid / 1,2-dichloro-ethane / 3 h / 20 °C

5.1: 100 percent / hydrogen / Pd(OH)2/C / ethyl acetate / 24 h / 20 °C

6.1: DMSO; (COCl)2; triethylamine / CH₂Cl₂ / 2.25 h / -80 - -60 °C

7.1: 4.8 g / toluene / 0.58 h / -80 - -70 °C

8.1: 3.79 g / NaH / tetrahydrofuran; dimethylformamide / 7 h / 20 °C

9.1: N-methylmorpholine N-oxide; OsO₄ / 2-methyl-propan-2-ol; H₂O / 24 h / 20 °C

10.1: NaIO₄ / 2-methyl-propan-2-ol; H₂O / 1 h / 20 °C

11.1: 437 mg / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 3 h / 20 °C

12.1: 75 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine; 10-camphorsulfonic acid / CH₂Cl₂ / 24 h / 35 °C

13.1: 63 percent / tetrahydrofuran / 60 °C

14.1: BH₃*THF / tetrahydrofuran / 0 - 20 °C

14.2: 75 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 0 - 20 °C

15.1: 57 percent / DMSO; (COCl)2; triethylamine / CH₂Cl₂ / 1.5 h / -70 - -40 °C

16.1: 58 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 12 h / 20 °C

17.1: 84 percent / trifluoromethanesulfonic acid / hexane / 19 h / 20 °C

18.1: 71 percent / Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / 1 h / -50 - -20 °C

19.1: 99 percent / hydrogen; AcOH / Pd(OH)2/C / ethyl acetate; methanol / 72 h / 20 °C

20.1: 174 mg / 10-camphorsulfonic acid / tetrahydrofuran / 1 h / 20 °C

21.1: 100 percent / N,N-diisopropylethylamine / 1,2-dichloro-ethane / 14 h / 40 °C

With triethylsilane; dmap; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; borane-THF; 2-methyl-but-2-ene; oxalyl dichloride; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; (1S)-10-camphorsulfonic acid; hydrogen; bis-(1,2-dimethylpropyl)borane; sodium hydride; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 6.1: Swern oxidation / 15.1: Swern oxidation;
DOI:10.1016/S0040-4020(02)00660-9

Reference yield:

: (E)-(R)-6-Benzyloxy-2,3-dimethyl-hex-4-enoic acid

: 474125-39-8
C₄₁H₅₆O₁₀

Guidance literature:: Multi-step reaction with 24 steps

1.1: 24.8 g / ethyl acetate / 0 - 20 °C

2.1: 62 percent / I₂ / acetonitrile / 0 - 20 °C

3.1: aq. NaOH / ethanol / 2 h / 20 °C

3.2: 72 percent / AcOH / ethanol / 1 h / 60 °C

4.1: 95 percent / N,N-diisopropylethylamine / 1,2-dichloro-ethane / 24 h / 50 °C

5.1: tetrahydrofuran / 1.17 h / -70 °C

6.1: disiamylborane / tetrahydrofuran / 1.17 h / 0 °C

6.2: H₂O₂; NaHCO₃ / tetrahydrofuran; methanol; H₂O / 20 °C

7.1: 37.5 g / 10-camphorsulfonic acid / 1,2-dichloro-ethane / 3 h / 20 °C

8.1: 100 percent / hydrogen / Pd(OH)2/C / ethyl acetate / 24 h / 20 °C

9.1: DMSO; (COCl)2; triethylamine / CH₂Cl₂ / 2.25 h / -80 - -60 °C

10.1: 4.8 g / toluene / 0.58 h / -80 - -70 °C

11.1: 3.79 g / NaH / tetrahydrofuran; dimethylformamide / 7 h / 20 °C

12.1: N-methylmorpholine N-oxide; OsO₄ / 2-methyl-propan-2-ol; H₂O / 24 h / 20 °C

13.1: NaIO₄ / 2-methyl-propan-2-ol; H₂O / 1 h / 20 °C

14.1: 437 mg / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 3 h / 20 °C

15.1: 75 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine; 10-camphorsulfonic acid / CH₂Cl₂ / 24 h / 35 °C

16.1: 63 percent / tetrahydrofuran / 60 °C

17.1: BH₃*THF / tetrahydrofuran / 0 - 20 °C

17.2: 75 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 0 - 20 °C

18.1: 57 percent / DMSO; (COCl)2; triethylamine / CH₂Cl₂ / 1.5 h / -70 - -40 °C

19.1: 58 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 12 h / 20 °C

20.1: 84 percent / trifluoromethanesulfonic acid / hexane / 19 h / 20 °C

21.1: 71 percent / Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / 1 h / -50 - -20 °C

22.1: 99 percent / hydrogen; AcOH / Pd(OH)2/C / ethyl acetate; methanol / 72 h / 20 °C

23.1: 174 mg / 10-camphorsulfonic acid / tetrahydrofuran / 1 h / 20 °C

24.1: 100 percent / N,N-diisopropylethylamine / 1,2-dichloro-ethane / 14 h / 40 °C

With triethylsilane; dmap; sodium hydroxide; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; borane-THF; 2-methyl-but-2-ene; oxalyl dichloride; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; (1S)-10-camphorsulfonic acid; hydrogen; iodine; bis-(1,2-dimethylpropyl)borane; sodium hydride; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 9.1: Swern oxidation / 18.1: Swern oxidation;
DOI:10.1016/S0040-4020(02)00660-9