3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

Base Information

Chemical Name:3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide
CAS No.:947530-63-4
Molecular Formula:C₁₇H₂₄BrNO₃Si
Molecular Weight:398.372
Hs Code.:

Synonyms:3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

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Technology Process of 3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

There total 2 articles about 3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 162330-95-2
β-(2-bromo-4,5-dimethoxyphenyl)-N-methylethylamine

: trimethylsilanyl-propynoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 947530-63-4
3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

Guidance literature:: In 1,4-dioxane; at 20 ℃;
DOI:10.1021/ol071079g

Reference yield:

: 5683-31-8
3-(trimethylsilyl)prop-2-ynoic acid

: 947530-63-4
3-trimethylsilylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / dioxane / 20 °C

2: 97 percent / dioxane / 20 °C

With dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ol071079g