C₂₆H₂₂ClNO₄

Base Information

• Chemical Name: C₂₆H₂₂ClNO₄
• CAS No.: 936566-16-4
• Molecular Formula: C₂₆H₂₂ClNO₄
• Molecular Weight: 447.918
• Mol file: 936566-16-4.mol

Synonyms:C₂₆H₂₂ClNO₄

Chemical Property of C₂₆H₂₂ClNO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₂ClNO₄

There total 1 articles about C₂₆H₂₂ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(E)-1-(3-chlorophenyl)-3-(4-methoxyphenyl)prop-2-en-1-one + 1H-[1]benzazepin-2,5(3H,4H)-dione (16511-38-9) → C26H22ClNO4 (936566-16-4)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; at 25 ℃; for 2h;

DOI:10.1016/j.bmcl.2007.01.043

Reference yield: 73.0%

C26H22ClNO4 (936566-16-4) → C26H19ClN2O2 (936566-30-2)

Guidance literature:

With ammonium iron(III) sulfate dodecahydrate; ammonium acetate; acetic acid; for 3h; Heating;

DOI:10.1016/j.bmcl.2007.01.043

Reference yield:

C26H22ClNO4 (936566-16-4) → C25H17ClN2O2 (936566-17-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 73 percent / ammonium ferric sulphate dodecahydrate; NH₄OAC; AcOH / 3 h / Heating

2.1: BBr₃ / CH₂Cl₂ / 2 h / 25 °C

2.2: 61 percent / H₂O / CH₂Cl₂ / 1 h

With ammonium iron(III) sulfate dodecahydrate; ammonium acetate; boron tribromide; acetic acid; In dichloromethane;

DOI:10.1016/j.bmcl.2007.01.043

upstream raw materials:

1H-[1]benzazepin-2,5(3H,4H)-dione

Downstream raw materials:

C₂₆H₁₉ClN₂O₂

C₂₅H₁₇ClN₂O₂

C₂₉H₂₄BrClN₂O₂

C₃₇H₂₈ClN₃O₄