1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione

Base Information

• Chemical Name: 1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione
• CAS No.: 1057661-48-9
• Molecular Formula: C₂₄H₂₈O₈
• Molecular Weight: 444.482

Synonyms:1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione

Chemical Property of 1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione

Chemical Property:

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Technology Process of 1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione

There total 1 articles about 1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-[2-(1,1-dimethyl-2-propynyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione (1057661-46-7) → 1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione (1057661-48-9)

Guidance literature:

With pyridine; Pd-BaSO₄; hydrogen; In dichloromethane; at 20 ℃; for 0.666667h; under 760.051 Torr;

DOI:10.1021/jo8013353

Reference yield: 14.0%

1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione (1057661-48-9) → C20H20O6 (1057661-52-5) + C20H20O6 (1057661-53-6) + licoagrodione

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 0.5h; Microwave irradiation;

DOI:10.1021/jo8013353

Reference yield:

1-[2-(1,1-dimethylallyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione (1057661-48-9) → C22H24O7 + C24H28O8

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1021/jo8013353

upstream raw materials:

1-[2-(1,1-dimethyl-2-propynyloxy)-4-methoxymethoxy-phenyl]-2-(4-methoxy-2-methoxymethoxy-phenyl)ethane-1,2-dione

Downstream raw materials:

C₂₀H₂₀O₆

C₂₀H₂₀O₆

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