2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

Base Information

Chemical Name:2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester
CAS No.:951330-14-6
Molecular Formula:C₃₄H₅₁N₃O₅
Molecular Weight:581.796
Hs Code.:

Synonyms:2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

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Chemical Property of 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

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Technology Process of 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

There total 5 articles about 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 19009-39-3
N,N-diisopropylcarbamoyl chloride

: 951330-00-0
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-hydroxypent-1-yl ester

: 951330-14-6
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 17h; Heating;
DOI:10.1055/s-2007-983724

Reference yield:

: C₃₃H₅₂N₂O₄Si

: 951330-14-6
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 10.45 g / TBAF / tetrahydrofuran / 72 h / 20 °C

2: 99 percent / NaH / tetrahydrofuran; various solvent(s) / 17 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1055/s-2007-983724

Reference yield:

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 951330-14-6
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylic acid (S)-2-(N,N-dibenzylamino)-5-(N,N-diisopropylcarbamoyloxy)pent-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran; various solvent(s) / 17 h / Heating

2: 10.45 g / TBAF / tetrahydrofuran / 72 h / 20 °C

3: 99 percent / NaH / tetrahydrofuran; various solvent(s) / 17 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1055/s-2007-983724