1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

Base Information

Chemical Name:1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester
CAS No.:127027-77-4
Molecular Formula:C₂₀H₂₀N₂O₇
Molecular Weight:400.388
Hs Code.:

Synonyms:1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

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Chemical Property of 1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

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Technology Process of 1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

There total 1 articles about 1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127027-75-2
Methyl-6-(benzyloxy)-2,3-dihydro-7-methoxyindol-2-carboxylat

: 127027-77-4
1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / AcONa / 1.5 h / 80 °C

2: 100 percent HNO₃, Ac₂O / 7 h / Ambient temperature

With nitric acid; sodium acetate; acetic anhydride;
DOI:10.1002/hlca.19890720717

Reference yield: 84.0%

: 127027-77-4
1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

: 156235-20-0
1-Acetyl-5-amino-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

Guidance literature:: With hydrogen; platinum on activated charcoal; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1002/hlca.19940770114

Reference yield:

: 127027-77-4
1-Acetyl-5-nitro-6-(benzyloxy)-2,3-dihydro-7-methoxy-1H-indol-2-carbonsaeure-methylester

: 156235-22-2
5-Amino-6-(benzyloxy)-7-methoxy-1H-indol-2-carbonsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / H₂ / 5percent Pt/C / tetrahydrofuran / 6 h / Ambient temperature

2: 94 percent / concd. HCl / methanol / 23 h / 50 °C

3: 65 percent / Cu(OAc)2*H₂O, air / ethyl acetate / 3 h / Ambient temperature

With hydrogenchloride; copper diacetate; air; hydrogen; platinum on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1002/hlca.19940770114