4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Base Information

Chemical Name:4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole
CAS No.:948854-57-7
Molecular Formula:C₁₈H₁₉N₃OSe
Molecular Weight:372.328
Hs Code.:

Synonyms:4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

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Chemical Property of 4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Chemical Property:

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Technology Process of 4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

There total 4 articles about 4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 879131-92-7
N-(3-phenylselanylpropionyl)hydrazine

: 948854-57-7
4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 0 - 20 °C

2: 1,2-dichloro-benzene / 3 h / Heating

With pyridine; In dichloromethane; 1,2-dichloro-benzene;
DOI:10.1016/j.tet.2007.05.080

Reference yield:

: 1666-13-3
diphenyl diselenide

: 948854-57-7
4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaBH₄ / tetrahydrofuran; dimethylformamide / 8 h / 20 °C

1.2: 100 percent / tetrahydrofuran; dimethylformamide / 4 h / 20 °C

2.1: hydrazine hydrate / methanol; H₂O / Heating

3.1: pyridine / CH₂Cl₂ / 0 - 20 °C

4.1: 1,2-dichloro-benzene / 3 h / Heating

With pyridine; sodium tetrahydroborate; hydrazine hydrate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene;
DOI:10.1016/j.tet.2007.05.080

Reference yield:

: 109179-39-7
Ethyl 3-(Phenylseleno)propionate

: 948854-57-7
4-(3-methoxy-phenyl)-3-methyl-5-(2-(phenylselanyl)ethyl)-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol; H₂O / Heating

2: pyridine / CH₂Cl₂ / 0 - 20 °C

3: 1,2-dichloro-benzene / 3 h / Heating

With pyridine; hydrazine hydrate; In methanol; dichloromethane; water; 1,2-dichloro-benzene;
DOI:10.1016/j.tet.2007.05.080