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propargyl ketone

Base Information
  • Chemical Name:propargyl ketone
  • CAS No.:1527481-05-5
  • Molecular Formula:C15H18O4
  • Molecular Weight:262.306
  • Hs Code.:
propargyl ketone

Synonyms:propargyl ketone

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Chemical Property of propargyl ketone
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Technology Process of propargyl ketone

There total 2 articles about propargyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In chloroform; dimethyl sulfoxide; for 2h; Reflux;
DOI:10.1016/j.tet.2013.11.060
Guidance literature:
Multi-step reaction with 2 steps
1: tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / chloroform; dimethyl sulfoxide / 2 h / Reflux
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; chloroform; dimethyl sulfoxide;
DOI:10.1016/j.tet.2013.11.060
Guidance literature:
Multi-step reaction with 2 steps
1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / chloroform; water / 2 h / Inert atmosphere; Reflux
2: lithium hydroxide / methanol / 1 h / 40 °C / Inert atmosphere
With copper(ll) sulfate pentahydrate; sodium L-ascorbate; lithium hydroxide; In methanol; chloroform; water;
DOI:10.1016/j.tet.2013.11.060
upstream raw materials:

5-isopropyl-2,3,4-trimethoxybenzaldehyde

C15H20O4

Downstream raw materials:

C19H25N3O6

C26H32N4O6

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