(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

Base Information

Chemical Name:(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate
CAS No.:1610376-73-2
Molecular Formula:C₁₆H₂₅O₃PS₂
Molecular Weight:360.478
Hs Code.:

Synonyms:(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

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Technology Process of (E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

There total 3 articles about (E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1610376-65-2
2-phenethyl-2-vinyloxirane

: 298-06-6
O,O-Diethyl hydrogen phosphorodithioate

: 1610376-70-9
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

: 1610376-73-2
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

Guidance literature:: In toluene; at 20 ℃; for 5h; Solvent; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 53931-59-2
5-phenyl-1-penten-3-one

: 1610376-70-9
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

: 1610376-73-2
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; diethyl ether / 0.37 h / -100 °C / Inert atmosphere

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

3: toluene / 5 h / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 1610376-87-8
C₁₂H₁₅ClO

: 1610376-70-9
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

: 1610376-73-2
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diethyl phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

2: toluene / 5 h / 20 °C / Inert atmosphere

With sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028