2,6-dimethyl 1-deuterio benzene

Base Information

• Chemical Name: 2,6-dimethyl 1-deuterio benzene
• CAS No.: 38422-51-4
• Molecular Formula: C₈H₁₀
• Molecular Weight: 107.159
• Mol file: 38422-51-4.mol

Synonyms:2,6-dimethyl 1-deuterio benzene

Chemical Property of 2,6-dimethyl 1-deuterio benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-dimethyl 1-deuterio benzene

There total 3 articles about 2,6-dimethyl 1-deuterio benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromo-m-xylene (576-22-7) → 2,6-dimethyl 1-deuterio benzene (38422-51-4)

Guidance literature:

With water-d2; magnesium; Yield given. Multistep reaction; 1.) THF, 2 h;

DOI:10.1021/ja00223a020

Reference yield:

m-xylene (108-38-3,104809-90-7) + trifluoroacetic acid (76-05-1) → 2,6-dimethyl 1-deuterio benzene (38422-51-4) + 2,4-dimethyl 1-deuterio benzene (106720-10-9)

Guidance literature:

at 70 ℃; Kinetics;

DOI:10.1021/ja01556a066

Reference yield:

→ 2,6-dimethyl 1-deuterio benzene (38422-51-4)

Guidance literature:

2-Bromo-m-xylol 1. ueber Grignard, 2. Zers. in D2O;

DOI:10.1021/jo00986a014

upstream raw materials:

2-Bromo-m-xylene

m-xylene

trifluoroacetic acid

Downstream raw materials:

1,3-bis(bromomethyl)-2-deuteriobenzene

C₆H₃D(CH₂N(C₂H₄C₅H₄N)2)2