2,6-Dichloro-4-methylnicotinaldehyde

Base Information

Chemical Name:2,6-Dichloro-4-methylnicotinaldehyde
CAS No.:91591-70-7
Molecular Formula:C7H5 Cl2 N O
Molecular Weight:190.03
Hs Code.:2933399090
DSSTox Substance ID:DTXSID70551195
Nikkaji Number:J1.369.526A
Wikidata:Q82430723
Mol file:91591-70-7.mol

Synonyms:2,6-DICHLORO-4-METHYLNICOTINALDEHYDE;91591-70-7;2,6-Dichloro-4-methylpyridine-3-carbaldehyde;2,6-Dichloro-4-methylpyridine-3-carboxaldehyde;SCHEMBL5871099;DTXSID70551195;MFCD11044320;AKOS006308095;AS-62768;CS-0096052;F12418;A860321

Suppliers and Price of 2,6-Dichloro-4-methylnicotinaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2,6-Dichloro-4-methylnicotinaldehyde 95+%
1g
$ 451.00

Chemenu
2,6-Dichloro-4-methylnicotinaldehyde 95%
1g
$ 426.00

American Custom Chemicals Corporation
2,6-DICHLORO-4-METHYLNICOTINALDEHYDE 95.00%
5MG
$ 502.03

American Custom Chemicals Corporation
2,6-DICHLORO-4-METHYLNICOTINALDEHYDE 95.00%
1G
$ 1000.65

Ambeed
2,6-Dichloro-4-methylnicotinaldehyde 95%
5g
$ 728.00

Ambeed
2,6-Dichloro-4-methylnicotinaldehyde 95%
250mg
$ 168.00

Ambeed
2,6-Dichloro-4-methylnicotinaldehyde 95%
1g
$ 342.00

Alichem
2,6-Dichloro-4-methylnicotinaldehyde
25g
$ 2759.12

Alichem
2,6-Dichloro-4-methylnicotinaldehyde
10g
$ 1459.26

Alichem
2,6-Dichloro-4-methylnicotinaldehyde
5g
$ 1168.48

Total 17 raw suppliers

Chemical Property of 2,6-Dichloro-4-methylnicotinaldehyde

Chemical Property:

PSA：29.96000
LogP:2.50930
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:188.9748192
Heavy Atom Count:11
Complexity:153

Purity/Quality:

97% ^*data from raw suppliers

2,6-Dichloro-4-methylnicotinaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=NC(=C1C=O)Cl)Cl

Technology Process of 2,6-Dichloro-4-methylnicotinaldehyde

There total 3 articles about 2,6-Dichloro-4-methylnicotinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1086322-08-8
(2,6-dichloro-4-methylpyridin-3-yl)methanol

: 91591-70-7
2,6-dichloro-4-methyl-3-pyridinecarboxaldehyde

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; at 25 ℃; for 2h;

Reference yield: 66.0%

: 875-35-4
2,6-dichloro-4-methylnicotinonitrile

: 91591-70-7
2,6-dichloro-4-methyl-3-pyridinecarboxaldehyde

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 - 20 ℃; for 2h;
DOI:10.1021/jo991886w

Reference yield:

: 62774-90-7
2,6-dichloro-4-methyl-nicotinic acid

: 91591-70-7
2,6-dichloro-4-methyl-3-pyridinecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 6 h / 20 °C

With borane-THF; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol402489e