para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:946076-04-6
Molecular Formula:C₁₀₁H₁₀₀N₂O₂₅
Molecular Weight:1741.9
Hs Code.:

para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Synonyms:para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 1 articles about para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946076-03-5
para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 946076-04-6
para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; for 55h;

Reference yield:

: 4'-pentenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-2)]-3,6-di-O-benzyl-α-D-mannopyranoside

: 946076-04-6
para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: para-methoxyphenyl {3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-2)]-3,6-di-O-benzyl-α-D-mannopyranosyl-(1-3)}-4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: 4'-pentenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-2)]-3,6-di-O-benzyl-α-D-mannopyranoside; para-methoxyphenyl 4,6-O-benzylidene-2-O-levulinoyl-β-D-glucopyranosyl-(1-4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1-4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1-6)]-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside; With N-iodo-succinimide; In dichloromethane; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 0.75h;