4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

Base Information

Chemical Name:4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene
CAS No.:194281-33-9
Molecular Formula:C₃₂H₃₄O₅
Molecular Weight:498.619
Hs Code.:

Synonyms:4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

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Chemical Property of 4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

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Technology Process of 4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

There total 9 articles about 4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethenyl]-2'-methoxydiphenylether

: 194281-33-9
4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 3800 Torr;

Reference yield: 82.0%

: C₃₂H₃₂O₅

: 194281-33-9
4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h; under 3750.3 Torr;
DOI:10.1016/S0031-9422(97)00118-0

Reference yield:

: 122849-97-2
(2,3-dimethoxybenzyl)triphenylphosphonium chloride

: 194281-33-9
4-[2-(3-methoxyphenyl)ethyl]-5'-[2-(2,3-dimethoxyphenyl)ethyl]-2'-methoxydiphenylethene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / K₂CO₃; 18-crown-6 / toluene / 18 h / Heating

2: 90 percent / hydrogen / Pd/C 10 percent / ethyl acetate / 3800 Torr

With 18-crown-6 ether; hydrogen; potassium carbonate; palladium on activated charcoal; In ethyl acetate; toluene;