4-acrylamido benzene sulphonyl guanidine

Base Information

• Chemical Name: 4-acrylamido benzene sulphonyl guanidine
• CAS No.: 1256381-10-8
• Molecular Formula: C₁₀H₁₂N₄O₃S
• Molecular Weight: 268.296
• Mol file: 1256381-10-8.mol

Synonyms:4-acrylamido benzene sulphonyl guanidine

Chemical Property of 4-acrylamido benzene sulphonyl guanidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-acrylamido benzene sulphonyl guanidine

There total 1 articles about 4-acrylamido benzene sulphonyl guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acryloyl chloride (814-68-6,25189-84-8) + 1-amino-4-({[amino(imino)methyl]amino}sulfonyl)benzene (57-67-0,61116-95-8) → 4-acrylamido benzene sulphonyl guanidine (1256381-10-8)

Guidance literature:

In benzene; at 0 ℃; Inert atmosphere;

DOI:10.1016/j.saa.2010.08.006

Reference yield:

nickel(II) iodide (13462-90-3) + 4-acrylamido benzene sulphonyl guanidine (1256381-10-8) → [(CH2CHCONHC6H4SO2NHC(NH2)NH)2NiI2]

Guidance literature:

With 2,2'-azobisisobutyronitrile; In N,N-dimethyl-formamide; refluxed for 8 h; pptd. by pouring in aq. HCl, filtered, washed (H2O), dried (vac., at 40°C, for days);

DOI:10.1016/j.molstruc.2011.01.015

Reference yield:

4-acrylamido benzene sulphonyl guanidine (1256381-10-8) + nickel(II) nitrate → [(CH2CHCONHC6H4SO2NHC(NH2)NH)2Ni(ONO2)2]

Guidance literature:

With 2,2'-azobisisobutyronitrile; In N,N-dimethyl-formamide; refluxed for 8 h; pptd. by pouring in aq. HCl, filtered, washed (H2O), dried (vac., at 40°C, for days);

DOI:10.1016/j.molstruc.2011.01.015

upstream raw materials:

acryloyl chloride

1-amino-4-({[amino(imino)methyl]amino}sulfonyl)benzene