C₄₁H₆₆O₅Si₂

Base Information

• Chemical Name: C₄₁H₆₆O₅Si₂
• CAS No.: 1435478-94-6
• Molecular Formula: C₄₁H₆₆O₅Si₂
• Molecular Weight: 695.143

Synonyms:C₄₁H₆₆O₅Si₂

Chemical Property of C₄₁H₆₆O₅Si₂

Chemical Property:

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Technology Process of C₄₁H₆₆O₅Si₂

There total 2 articles about C₄₁H₆₆O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C41H68O5Si2 (1435478-38-8) → C41H66O5Si2 (1435478-94-6)

Guidance literature:

With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 0 ℃; for 1h;

DOI:10.1039/c3ob40131f

Reference yield:

C48H74O5Si2 → C41H66O5Si2 (1435478-94-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol; ethyl acetate

2: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

With 10 wt% Pd(OH)2 on carbon; hydrogen; sulfur trioxide pyridine complex; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate;

DOI:10.1039/c3ob40131f

Reference yield:

C21H23IN4O4S (1207069-42-8) + C41H66O5Si2 (1435478-94-6) → C55H83IO6Si2 (1435478-39-9) + C55H83IO6Si2 (1435478-96-8)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 0 ℃; Overall yield = 88 %; Overall yield = 462 mg;

DOI:10.1039/c3ob40131f

upstream raw materials:

C₄₁H₆₈O₅Si₂

Downstream raw materials:

C₅₅H₈₃IO₆Si₂

C₅₅H₈₃IO₆Si₂

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