C₁₀H₁₀BrNO₂

Base Information

Chemical Name:C₁₀H₁₀BrNO₂
CAS No.:1420013-02-0
Molecular Formula:C₁₀H₁₀BrNO₂
Molecular Weight:256.099
Hs Code.:

C<sub>10</sub>H<sub>10</sub>BrNO<sub>2</sub>

Synonyms:C₁₀H₁₀BrNO₂

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Chemical Property of C₁₀H₁₀BrNO₂

Chemical Property:

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Technology Process of C₁₀H₁₀BrNO₂

There total 8 articles about C₁₀H₁₀BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420013-09-7
N-(2-bromo-3-(2-methoxyvinyl)phenyl)acetamide

: 1420013-02-0
C₁₀H₁₀BrNO₂

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja3121394

Reference yield:

: 573-54-6
2-bromo-3-nitro-benzoic acid

: 1420013-02-0
C₁₀H₁₀BrNO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: borane-THF / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.1: acetic acid; iron; hydrogenchloride / ethanol / 3 h / 100 °C

3.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: manganese(IV) oxide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

7.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

7.2: 0.25 h / Inert atmosphere

8.1: hydrogenchloride / tetrahydrofuran / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; dmap; manganese(IV) oxide; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; iron; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja3121394

Reference yield:

: 90407-20-8
2-bromo-3-(hydroxymethyl)-1-nitrobenzene

: 1420013-02-0
C₁₀H₁₀BrNO₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: acetic acid; iron; hydrogenchloride / ethanol / 3 h / 100 °C

2.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: manganese(IV) oxide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

6.2: 0.25 h / Inert atmosphere

7.1: hydrogenchloride / tetrahydrofuran / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; hydrogenchloride; dmap; manganese(IV) oxide; potassium tert-butylate; tetrabutyl ammonium fluoride; iron; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja3121394