(CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)

Base Information

Chemical Name:(CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)
CAS No.:881914-03-0
Molecular Formula:C₃₆H₃₄IrN₂O₂P₂RhSi
Molecular Weight:911.837
Hs Code.:

Synonyms:(CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)

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Technology Process of (CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)

There total 1 articles about (CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 881913-65-1
[(CO)2Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)2]BF₄

: 1066-54-2
trimethylsilylacetylene

: 881914-03-0
(CO)Rh(3,5-bis((diphenylphosphino)methyl)pyrazolato)Ir(CO)(μ-CCSiMe3)

Guidance literature:: With n-BuLi; In tetrahydrofuran; under inert atm. to soln. HCCSiMe3 in THF at -75°C n-BuLi was added, after 10 min soln. Rh-Ir complex in THF was added and stirred for 10min at -75°C, for 30 min at 0°C, and for 1 h at room temp .; soln. was filtered through alumina and concd. in vacuo, Et2O was added;
DOI:10.1021/om050897e