Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)

Base Information

Chemical Name:Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)
CAS No.:91531-61-2
Molecular Formula:C₁₀H₁₄O
Molecular Weight:150.221
Hs Code.:
Mol file:91531-61-2.mol

Synonyms:Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)

Suppliers and Price of Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)

Chemical Property:

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Technology Process of Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI)

There total 2 articles about Cyclobutanol, 1-ethynyl-2-(2-methyl-1-propenyl)-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1-(trimethylsilylethynyl)-2-(2'-methyl-1'-propenyl)cyclobutanol

: 344770-94-1,91531-47-4,91531-61-2
1-ethynyl-2-(2'-methyl-1'-propenyl)cyclobutanol

Guidance literature:: With potassium hydroxide; In 1,2-dimethoxyethane; for 0.333333h; Ambient temperature;
DOI:10.1002/hlca.19840670319

Reference yield:

: 91531-45-2
2-(2'-methyl-1'-propenyl)cyclobutanone

: 344770-94-1,91531-47-4,91531-61-2
1-ethynyl-2-(2'-methyl-1'-propenyl)cyclobutanol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 1,2-dimethoxy-ethane / 3 h

2: 90 percent / 5percent aq. KOH / 1,2-dimethoxy-ethane / 0.33 h / Ambient temperature

With potassium hydroxide; In 1,2-dimethoxyethane;
DOI:10.1002/hlca.19840670319