Technology Process of methyl 2,6-di-O-benzyl-3-O-methyl-β-D-galactopyranoside
There total 8 articles about methyl 2,6-di-O-benzyl-3-O-methyl-β-D-galactopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; molecular sieve; sodium cyanoborohydride;
In
tetrahydrofuran;
Ambient temperature;
DOI:10.1016/S0008-6215(00)90292-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / toluene-p-sulfonic acid / acetonitrile / 16 h / Ambient temperature
2: 30 percent / 1.25M sodium hydroxide, tetrabutylammonium hydrogensulfate / CH2Cl2 / 24 h / Heating
3: 90 percent / sodium methylsulfinylmethanide / 4 h / Ambient temperature
4: 78 percent / ethereal hydrogen chloride, sodium cyanoborohydride, molecular sieves / tetrahydrofuran / Ambient temperature
With
hydrogenchloride; sodium hydroxide; molecular sieve; tetra(n-butyl)ammonium hydrogensulfate; sodium cyanoborohydride; sodium methylsulfinylmethanide; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(00)90292-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / toluene-p-sulfonic acid / acetonitrile / 16 h / Ambient temperature
2: 30 percent / 1.25M sodium hydroxide, tetrabutylammonium hydrogensulfate / CH2Cl2 / 24 h / Heating
3: 90 percent / sodium methylsulfinylmethanide / 4 h / Ambient temperature
4: 78 percent / ethereal hydrogen chloride, sodium cyanoborohydride, molecular sieves / tetrahydrofuran / Ambient temperature
With
hydrogenchloride; sodium hydroxide; molecular sieve; tetra(n-butyl)ammonium hydrogensulfate; sodium cyanoborohydride; sodium methylsulfinylmethanide; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0008-6215(00)90292-1
