Technology Process of C15H16INO2S2
There total 5 articles about C15H16INO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ol303366u
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine
2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: potassium carbonate / methanol / 20 °C / Inert atmosphere
With
pyridine; sodium hydride; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol303366u
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine
2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: potassium carbonate / methanol / 20 °C / Inert atmosphere
With
pyridine; sodium hydride; potassium carbonate; caesium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol303366u