N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide
CAS No.:1252643-49-4
Molecular Formula:C₂₈H₃₃F₁₁N₄O₅S
Molecular Weight:746.642
Hs Code.:

N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

Synonyms:N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

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Chemical Property of N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

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Technology Process of N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

There total 3 articles about N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 354-38-1
2,2,2-trifluoroacetamide

: 1252642-89-9
5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-1-{9-[(4,4,5,5,5-pentafluoropentyl)thio]nonyl}imidazolidine-2,4-dione

: 1252643-49-4
N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: With [bis(acetoxy)iodo]benzene; magnesium oxide; dirhodium tetraacetate; In dichloromethane; at 23 ℃; for 6h;

Reference yield:

: 63612-50-0
nilutamide

: 1252643-49-4
N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere

1.2: 15 h / Inert atmosphere

2.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 6 h / 23 °C

With [bis(acetoxy)iodo]benzene; magnesium oxide; sodium hydride; dirhodium tetraacetate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 862700-62-7
methanesulfonic acid 9-(4,4,5,5,5-pentafluoro-pentyl-sulfanyl)-nonyl ester

: 1252643-49-4
N-[(1Z)-(9-{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]-2,4-dioxoimidazolidin-1-yl}nonyl)(4,4,5,5,5-pentafluoropentyl)-λ4-sulphanylidene]-2,2,2-trifluoroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 23 °C / Inert atmosphere

1.2: 15 h / Inert atmosphere

2.1: magnesium oxide; [bis(acetoxy)iodo]benzene / dirhodium tetraacetate / dichloromethane / 6 h / 23 °C

With [bis(acetoxy)iodo]benzene; magnesium oxide; sodium hydride; dirhodium tetraacetate; In dichloromethane; N,N-dimethyl-formamide;