carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

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Chemical Name:carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester
CAS No.:1196064-29-5
Molecular Formula:C₃₆H₅₃NO₅Si₂
Molecular Weight:635.992
Hs Code.:

Synonyms:carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

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Chemical Property of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

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Technology Process of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

There total 1 articles about carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1196064-28-4
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-hydroxynon-3-enyl ester

: 1196064-29-5
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1055/s-0029-1216921

Reference yield: 54.0%

: 1196064-23-9
methyl (2E,4R,5R,7E)-5-{2-[(diethoxy)phosphoryl]acetoxy}-8-iodo-2,4,7-trimethylocta-2,7-dienoate

: 1196064-29-5
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester

: C₅₀H₇₃NO₈Si₂

: 1196064-35-3
C₅₀H₇₃NO₈Si₂

Guidance literature:: carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-oxonon-3-enyl ester; With bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride; In tetrahydrofuran; for 1.83333h; Inert atmosphere;

methyl (2E,4R,5R,7E)-5-{2-[(diethoxy)phosphoryl]acetoxy}-8-iodo-2,4,7-trimethylocta-2,7-dienoate; With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 4h; Inert atmosphere;

With dichloro bis(acetonitrile) palladium(II); trifuran-2-yl-phosphane; lithium chloride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216921