N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

Base Information

Chemical Name:N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine
CAS No.:894392-60-0
Molecular Formula:C₆₇H₆₈N₂O₁₅
Molecular Weight:1141.28
Hs Code.:

N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

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Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

There total 7 articles about N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 894392-46-2
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine allyl ester

: 894392-60-0
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

Guidance literature:: With dimedone; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1271/bbb.69.1575

Reference yield:

: 894392-00-8
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine allyl ester

: 894392-60-0
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

Guidance literature:: Multi-step reaction with 3 steps

1: Zn; AcOH / CH₂Cl₂ / 3 h

2: 50 mg / methanol; CH₂Cl₂ / 1 h

3: 100 percent / 5,5-dimethyl-1,3-cyclohexanedione / Pd(Ph₃P)4 / tetrahydrofuran / 1.5 h / 20 °C

With dimedone; acetic acid; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1271/bbb.69.1575

Reference yield:

: C₆₈H₇₀N₂O₁₄

: 894392-60-0
N-(9-fluorenylmethoxycarbonyl)-O-[2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->3)-2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl]-L-serine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 mg / methanol; CH₂Cl₂ / 1 h

2: 100 percent / 5,5-dimethyl-1,3-cyclohexanedione / Pd(Ph₃P)4 / tetrahydrofuran / 1.5 h / 20 °C

With dimedone; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1271/bbb.69.1575