methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

Base Information

Chemical Name:methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate
CAS No.:1450658-22-6
Molecular Formula:C₁₈H₁₈N₂O₂
Molecular Weight:294.353
Hs Code.:

Synonyms:methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

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Chemical Property of methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

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Technology Process of methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

There total 1 articles about methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.7%

: 1450658-21-5
methyl 2-methyl-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 1450658-22-6
methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

Guidance literature:: methyl 2-methyl-1H-pyrrolo[2,3-b]pyridine-3-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

(1-bromoethyl)benzne; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h;

Reference yield: 84.0%

: 1450658-22-6
methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

: 1450658-23-7
2-methyl-1-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 60 ℃; for 48h;

Reference yield:

: 1450658-22-6
methyl 2-methyl-(1-phenylethyl)-1H-pyrrolo[2,3-b]pyridine-3-carboxylate

: 1450652-18-2
N-((2-hydroxy-4,6-dimethylpyridin-3-yl)methyl)-2-methyl-1-(1-phenylethyl)-1H-pyrrolo-[2,3-b]pyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 48 h / 60 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 0.5 h / 20 °C

2.2: 16 h / 20 °C

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;