ethyl 2-mercapto-5-methylcinnamate

Base Information

• Chemical Name: ethyl 2-mercapto-5-methylcinnamate
• CAS No.: 81536-26-7
• Molecular Formula: C₁₂H₁₄O₂S
• Molecular Weight: 222.308
• Mol file: 81536-26-7.mol

Synonyms:ethyl 2-mercapto-5-methylcinnamate

Chemical Property of ethyl 2-mercapto-5-methylcinnamate

Chemical Property:

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Technology Process of ethyl 2-mercapto-5-methylcinnamate

There total 1 articles about ethyl 2-mercapto-5-methylcinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

3,3,3-triethoxypropyne (42217-00-5) + para-thiocresol (106-45-6) → ethyl 2-mercapto-5-methylcinnamate (81536-26-7)

Guidance literature:

With Trimethylacetic acid; In various solvent(s); for 26h; Heating;

DOI:10.1021/jo00134a022

Reference yield: 90.0%

ethyl 2-mercapto-5-methylcinnamate (81536-26-7) → 2-mercapto-5-methylcinnamic acid (81536-31-4)

Guidance literature:

With potassium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1021/jo00134a022

upstream raw materials:

3,3,3-triethoxypropyne

para-thiocresol

Downstream raw materials:

2-mercapto-5-methylcinnamic acid