C₁₅H₂₇NOSi

Base Information

Chemical Name:C₁₅H₂₇NOSi
CAS No.:1316170-91-8
Molecular Formula:C₁₅H₂₇NOSi
Molecular Weight:265.471
Hs Code.:

Synonyms:C₁₅H₂₇NOSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₇NOSi

Chemical Property:

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Technology Process of C₁₅H₂₇NOSi

There total 1 articles about C₁₅H₂₇NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 182681-88-5
(2R)-1-cyano-2-hydroxy-4-pentyne

: 1316170-91-8
C₁₅H₂₇NOSi

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol201748x

Reference yield:

: 1316170-91-8
C₁₅H₂₇NOSi

: C₂₁H₃₄O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / toluene / 2 h / -52 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With diisobutylaluminium hydride; Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; toluene; 2.2: Aldol addition;
DOI:10.1021/ol201748x

Reference yield:

: 1316170-91-8
C₁₅H₂₇NOSi

: 1316170-96-3
C₂₁H₃₆O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / toluene / 2 h / -52 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: Inert atmosphere

With diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; toluene; 2.2: Aldol addition;
DOI:10.1021/ol201748x