(13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol

Base Information

Chemical Name:(13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol
CAS No.:75657-53-3
Molecular Formula:C₂₇H₄₀O₃
Molecular Weight:412.613
Hs Code.:
Mol file:75657-53-3.mol

Synonyms:16,24-Cyclo-13,17-secochola-16,20(22),23-triene-3,23-diol,14,17-epoxy-4,4,8-trimethyl-, (3b,5a,13a)-; (-)-Stypodiol; (-)-Stypoldiol; Stypodiol;Stypoldiol

Suppliers and Price of (13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol

Chemical Property:

PSA：49.69000
LogP:6.02390

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol

There total 63 articles about (13S)-14,17-Epoxy-4,4,8-trimethyl-16,24-cyclo-13,17-seco-5α-chola-16,20(22),23-triene-3β,23-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 149051-06-9
(1'S,2'S,4a'R,4b'S,7'S,8a'S,10a'R)-7'-(Benzoyloxy)-3',4'4a',4b',5',6',7',8',8a',9',10',10a'-dodecahydro-2',4b',7,8',8',10a'-hexamethylspiro-5-ol

: 75657-53-3
stypodiol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield: 86.0%

: 182880-85-9
(5α,13α)-14,17-epoxy-23-hydroxy-4,4,8-trimethyl-16,24-cyclo-13,17-secochola-16,20(22),23-trien-3-one

: 75657-53-3
stypodiol

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -60 - -10 ℃; for 1h;
DOI:10.1021/jo980311g

Reference yield:

: C₃₄H₄₄O₃

: 75657-53-3
stypodiol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 23 ℃; for 6h; under 2068.6 Torr; Yield given;
DOI:10.1021/ja00077a073