N-Trityldehydroalanine benzyl ester

Base Information

Chemical Name:N-Trityldehydroalanine benzyl ester
CAS No.:157552-57-3
Molecular Formula:C₂₉H₂₅NO₂
Molecular Weight:419.523
Hs Code.:

Synonyms:N-Trityldehydroalanine benzyl ester

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Chemical Property of N-Trityldehydroalanine benzyl ester

Chemical Property:

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Technology Process of N-Trityldehydroalanine benzyl ester

There total 5 articles about N-Trityldehydroalanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 153617-40-4
(S)-N-Trityl-β-chloroalanine benzyl ester

: 157552-57-3
N-Trityldehydroalanine benzyl ester

Guidance literature:: potassium fluoride; In N,N-dimethyl-formamide; at 90 ℃; for 4h;
DOI:10.1039/a909140h

Reference yield:

: 76-83-5
trityl chloride

: 157552-57-3
N-Trityldehydroalanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: 98 percent / KF / dimethylformamide / 4 h / 90 °C

With triethylamine; potassium fluoride; In dichloromethane; N,N-dimethyl-formamide; 1: Substitution / 2: Dehydrochlorination;
DOI:10.1039/a909140h

Reference yield:

: 263402-36-4
(S)-β-Chloroaniline benzyl ester

: 157552-57-3
N-Trityldehydroalanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: 98 percent / KF / dimethylformamide / 4 h / 90 °C

With triethylamine; potassium fluoride; In dichloromethane; N,N-dimethyl-formamide; 1: Substitution / 2: Dehydrochlorination;
DOI:10.1039/a909140h