1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol

Base Information

• Chemical Name: 1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol
• CAS No.: 1181208-83-2
• Molecular Formula: C₃₇H₄₀O₆
• Molecular Weight: 580.721

Synonyms:1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol

Chemical Property of 1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol

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Technology Process of 1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol

There total 1 articles about 1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

α,α'-dibromo-o-xylene (91-13-4) + (3S,4R,5S,6R)-3,5-dibenzyloxy-4,7-dihydroxy-6-(4-methoxybenzyl)oxyhept-1-ene (669053-65-0) → 1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol (1181208-83-2)

Guidance literature:

(3S,4R,5S,6R)-3,5-dibenzyloxy-4,7-dihydroxy-6-(4-methoxybenzyl)oxyhept-1-ene; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h;

α,α'-dibromo-o-xylene; In N,N-dimethyl-formamide; mineral oil; at 20 - 100 ℃;

Reference yield: 85.0%

1,2-dideoxy-6-O-(4-methoxybenzyl)-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol (1181208-83-2) → 1,2-dideoxy-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol (1181208-84-3)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 ℃; for 1.5h; pH=7.41;

upstream raw materials:

α,α'-dibromo-o-xylene

(3S,4R,5S,6R)-3,5-dibenzyloxy-4,7-dihydroxy-6-(4-methoxybenzyl)oxyhept-1-ene

Downstream raw materials:

1,2-dideoxy-3,5-di-O-benzyl-4,7-O-(o-xylylene)-D-gluco-hept-1-enitol

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