6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol

Base Information

• Chemical Name: 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol
• CAS No.: 1173165-12-2
• Molecular Formula: C₂₀H₂₃NO₄S
• Molecular Weight: 373.473

Synonyms:6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol

Chemical Property of 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol

Chemical Property:

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Technology Process of 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol

There total 1 articles about 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-[1-(benzyloxy)but-3-en-2-yl]-N-(2-hydroxybut-3-en-1-yl)-4-methylbenzenesulfonamide (1173165-09-7) → 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol (1173165-12-2)

Guidance literature:

With Hoveyda-Grubbs catalyst second generation; In dichloromethane; Reflux;

DOI:10.1016/j.tet.2009.07.076

Reference yield: 85.0%

6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]l-1,2,3,6-tetrahydropyridin-3-ol (1173165-12-2) → 6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]-1,6-dihydropyridin-3(2H)-one (1173165-15-5)

Guidance literature:

With Jones reagent; In acetone; at 0 ℃;

DOI:10.1039/b904363b

upstream raw materials:

N-[1-(benzyloxy)but-3-en-2-yl]-N-(2-hydroxybut-3-en-1-yl)-4-methylbenzenesulfonamide

Downstream raw materials:

6-[(benzyloxy)methyl]-1-[(4-methylphenyl)sulfonyl]-1,6-dihydropyridin-3(2H)-one

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