4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

Base Information

Chemical Name:4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime
CAS No.:705966-86-5
Molecular Formula:C₂₄H₁₄F₅NO₂
Molecular Weight:443.373
Hs Code.:

Synonyms:4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

Suppliers and Price of 4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

There total 1 articles about 4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1817-57-8
4-phenyl-3-butyne-2-one

: 705966-86-5
4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.83 h / -78 °C

1.2: 40 percent / tetrahydrofuran / 1.5 h / -78 - 20 °C

2.1: pyridine; hydroxylamine hydrochloride / ethanol / 12 h / 60 °C

3.1: 89 percent / triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

With pyridine; hydroxylamine hydrochloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1246/bcsj.77.785

Reference yield: 89.0%

: 705966-86-5
4-(cyclohepta-2,4,6-trienyl)-1-phenylbut-1-yn-3-one (Z)-O-pentafluorobenzoyloxime

: 13509-88-1
1-pentafluorophenyl-2-phenylacetylene

: 65810-22-2
1-(cyclohepta-2,4,6-trienyl)acetonitrile

Guidance literature:: With tri-tert-butyl phosphine; 4 A molecular sieve; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene; at 80 ℃; for 1h;
DOI:10.1246/bcsj.77.785