C₆₄H₈₂N₄O₁₂SSi

Base Information

Chemical Name:C₆₄H₈₂N₄O₁₂SSi
CAS No.:360787-60-6
Molecular Formula:C₆₄H₈₂N₄O₁₂SSi
Molecular Weight:1159.53
Hs Code.:

C<sub>64</sub>H<sub>82</sub>N<sub>4</sub>O<sub>12</sub>SSi

Synonyms:C₆₄H₈₂N₄O₁₂SSi

Suppliers and Price of C₆₄H₈₂N₄O₁₂SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₄H₈₂N₄O₁₂SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₄H₈₂N₄O₁₂SSi

There total 16 articles about C₆₄H₈₂N₄O₁₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [3-(1H-Indol-3-yl)-propyl]-[1-phenyl-meth-(E)-ylidene]-amine

: 360787-60-6
C₆₄H₈₂N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium borohydride / methanol / 0.42 h / 0 °C

2.1: 95 percent / NaOH / tetrahydrofuran / 3 h / 20 °C

3.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h

3.2: ZnCl₂ / tetrahydrofuran / 0.08 h

3.3: 89 percent / tetrahydrofuran / -60 - 20 °C

4.1: 96 percent / HCl / methanol / 2 h / 40 °C

5.1: 71 percent / toluene / 5 h / Heating

6.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating

7.1: NaBH₄ / NiCl₂

8.1: 97 percent / toluene / 18 h / Heating

9.1: triethylamine; tert-butyl hypochlorite / CH₂Cl₂ / 0 °C

10.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h

11.1: 361 mg / potassium borohydride / acetic acid / 0.17 h

With Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium hydroxide; sodium tetrahydroborate; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; toluene;
DOI:10.1021/jo000249z

Reference yield:

: 87400-38-2
N-benzyl-3-(1H-indol-3-yl)propan-1-amine

: 360787-60-6
C₆₄H₈₂N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 10 steps

1.1: 95 percent / NaOH / tetrahydrofuran / 3 h / 20 °C

2.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h

2.2: ZnCl₂ / tetrahydrofuran / 0.08 h

2.3: 89 percent / tetrahydrofuran / -60 - 20 °C

3.1: 96 percent / HCl / methanol / 2 h / 40 °C

4.1: 71 percent / toluene / 5 h / Heating

5.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating

6.1: NaBH₄ / NiCl₂

7.1: 97 percent / toluene / 18 h / Heating

8.1: triethylamine; tert-butyl hypochlorite / CH₂Cl₂ / 0 °C

9.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h

10.1: 361 mg / potassium borohydride / acetic acid / 0.17 h

With Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium hydroxide; sodium tetrahydroborate; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; toluene;
DOI:10.1021/jo000249z

Reference yield:

: 360788-10-9
benzyl-[3-(1H-indol-3-yl)-propyl]-carbamic acid tert-butyl ester

: 360787-60-6
C₆₄H₈₂N₄O₁₂SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine; tert-butyl hypochlorite / tetrahydrofuran / 0.33 h

1.2: ZnCl₂ / tetrahydrofuran / 0.08 h

1.3: 89 percent / tetrahydrofuran / -60 - 20 °C

2.1: 96 percent / HCl / methanol / 2 h / 40 °C

3.1: 71 percent / toluene / 5 h / Heating

4.1: 76 percent / Lawesson's reagent / toluene / 12 h / Heating

5.1: NaBH₄ / NiCl₂

6.1: 97 percent / toluene / 18 h / Heating

7.1: triethylamine; tert-butyl hypochlorite / CH₂Cl₂ / 0 °C

8.1: tetrafluoroboric acid-diethyl ether complex; silver tetrafluoroborate / acetone / 0.08 h

9.1: 361 mg / potassium borohydride / acetic acid / 0.17 h

With Lawessons reagent; hydrogenchloride; tetrafluoroboric acid diethyl ether; sodium tetrahydroborate; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; toluene;
DOI:10.1021/jo000249z