(R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

Base Information

Chemical Name:(R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester
CAS No.:1173893-43-0
Molecular Formula:C₂₁H₂₈BrNO₄
Molecular Weight:438.362
Hs Code.:

Synonyms:(R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

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Technology Process of (R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

There total 1 articles about (R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1173893-42-9
(R)-2-allyl-4-(4-bromophenyl)-2-tert-butoxycarbonylamino-pent-4-enoic acid tert-butyl ester

: 1173893-43-0
(R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.04.099

Reference yield: 54.0%

: 28741-08-4
n-octylboronic acid

: 1173893-43-0
(R)-3-(4-bromophenyl)-1-tert-butoxycarbonylaminocyclopent-3-enecarboxylic acid tert-butyl ester

: 1173893-44-1
(R)-1-tert-butoxycarbonylamino-3-(4-octylphenyl)cyclopent-3-enecarboxylic acid tert-butyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; at 110 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.04.099